tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

Base Information

Chemical Name:tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate
CAS No.:1224714-44-6
Molecular Formula:C₃₁H₅₁NO₅
Molecular Weight:517.75
Hs Code.:

Synonyms:tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

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Chemical Property of tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

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Technology Process of tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

There total 1 articles about tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1224714-43-5
tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enylcarbamate

: 74-88-4
methyl iodide

: 1224714-44-6
tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

Guidance literature:: tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.034

Reference yield: 79.0%

: 1224714-44-6
tert-butyl (1S,2R,5E,7R,9R)-1-[4-(allyloxy)benzyl]-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

: 1224714-45-7
tert-butyl (1S,2R,5E,7R,9R)-1-(4-hydroxybenzyl)-2-(methoxymethoxy)-7,9-dimethylundec-5-enyl(methyl)carbamate

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2010.02.034