N₆-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride

Base Information

• Chemical Name: N₆-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride
• CAS No.: 1310538-00-1
• Molecular Formula: C₁₃H₁₈ClN₅*ClH
• Molecular Weight: 316.233

Synonyms:N₆-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride

Chemical Property of N₆-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₆-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride

There total 2 articles about N₆-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N1-(4-chloro)phenethyl biguanide hydrochloride (110181-28-7) + acetone (67-64-1) → N6-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride (1310538-00-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; at 85 ℃; for 0.5h; Microwave irradiation;

DOI:10.1016/j.ejmech.2011.02.054

Reference yield:

4-chlorophenylethylamine (156-41-2) → N6-(4-chlorophenethyl)-2,2-dimethyl-1,2-dihydro-1,3,5-triazine-4,6-diamine hydrochloride (1310538-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride / tetrahydrofuran

1.2: 20 - 140 °C

2.1: hydrogenchloride / 1,4-dioxane; water / 0.5 h / 85 °C / Microwave irradiation

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; water;

DOI:10.1016/j.ejmech.2011.02.054

upstream raw materials:

N₁-(4-chloro)phenethyl biguanide hydrochloride

acetone

4-chlorophenylethylamine

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