1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol

Base Information

Chemical Name:1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol
CAS No.:145793-98-2
Molecular Formula:C₄₁H₄₆O₇
Molecular Weight:650.812
Hs Code.:

Synonyms:1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol

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Chemical Property of 1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol

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Technology Process of 1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol

There total 17 articles about 1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 162991-58-4
1D-1,4-di-O-allyl-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-myo-inositol

: 145793-98-2
1D-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-(cis-prop-1-enyl)-myo-inositol

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 50 ℃; for 9h;
DOI:10.1016/0008-6215(94)84005-9

Reference yield:

: 112204-05-4,149057-08-9
(+/-)-3,6-di-O-allyl-1,2-O-cyclohexylidene-myo-inositol

: 145793-98-2,145920-21-4
(+/-)-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-trans-prop-1-enyl-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: 53 percent / tetrabutylammonium hydrogen sulfate, 5percent aq. NaOH / CH₂Cl₂ / 24 h / Heating

2: NaH / dimethylformamide / 2 h / 20 °C

3: HCl / methanol / 5 h / 20 °C

4: 95 percent / NaH / dimethylformamide / 2 h / 20 °C

5: (1,5-cyclooctadiene)bis(methyldiphenylphosphine)iridium hexafluorophosphate / 1,2-dichloro-ethane / 4 h

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; (1,5-cyclooctadiene)bis(methyldiphenylphosphine)iridium hexafluorophosphate; In methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(92)85037-Z

Reference yield:

: 138328-96-8,149056-94-0
(+/-)-1,4-di-O-allyl-6-O-benzyl-5-O-p-methoxybenzyl-myo-inositol

: 145793-98-2,145920-21-4
(+/-)-2,3,6-tri-O-benzyl-5-O-p-methoxybenzyl-1,4-di-O-trans-prop-1-enyl-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaH / dimethylformamide / 2 h / 20 °C

2: (1,5-cyclooctadiene)bis(methyldiphenylphosphine)iridium hexafluorophosphate / 1,2-dichloro-ethane / 4 h

With sodium hydride; (1,5-cyclooctadiene)bis(methyldiphenylphosphine)iridium hexafluorophosphate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(92)85037-Z