ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate

Base Information

• Chemical Name: ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate
• CAS No.: 807380-63-8
• Molecular Formula: C₃₆H₃₉NO₇
• Molecular Weight: 597.708

Synonyms:ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate

Chemical Property of ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate

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Technology Process of ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate

There total 2 articles about ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.1%

6-nitroveratrylbromide (53413-67-5) + ethyl 4-[(E)-2-[3-(1-adamantyl)-4-hydroxyphenyl]ethenyl]benzoate (171365-87-0) → ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate (807380-63-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 12h;

DOI:10.1016/j.bmc.2004.08.022

Reference yield:

4-[(E)-2-(3-(1-adamantyl)-4-hydroxyphenyl)ethenyl]benzoic acid (146965-79-9) → ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate (807380-63-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 85.6 percent / H₂SO₄ / 12 h / Heating

2: 83.1 percent / K₂CO₃ / dimethylformamide / 12 h

With sulfuric acid; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2004.08.022

Reference yield: 75.1%

ethyl 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoate (807380-63-8) → 4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoic acid (807380-26-3)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 6h;

DOI:10.1016/j.bmc.2004.08.022

upstream raw materials:

6-nitroveratrylbromide

ethyl 4-[(E)-2-[3-(1-adamantyl)-4-hydroxyphenyl]ethenyl]benzoate

4-[(E)-2-(3-(1-adamantyl)-4-hydroxyphenyl)ethenyl]benzoic acid

Downstream raw materials:

4-[(E)-2-[3-(1-adamantyl)-4-[(nitroveratryl)oxy]phenyl]ethenyl]benzoic acid

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