N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine

Base Information

• Chemical Name: N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine
• CAS No.: 1015164-91-6
• Molecular Formula: C₂₁H₂₁N₃O₆
• Molecular Weight: 411.414
• Mol file: 1015164-91-6.mol

Synonyms:N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine

Chemical Property of N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine

There total 2 articles about N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

succinic acid anhydride (108-30-5) + 2-amino-N′-phenylbenzamidine (951-48-4) → C21H21N3O6 (1015164-91-6)

Guidance literature:

With sodium acetate; In acetic acid; for 3h; Heating;

DOI:10.1016/j.saa.2007.04.007

Reference yield: 83.0%

succinic acid anhydride (108-30-5) + 2-amino-N′-phenylbenzamidine (951-48-4) → N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine (1015164-91-6)

Guidance literature:

With sodium acetate; In acetic acid; for 3h; Heating;

DOI:10.1016/j.saa.2007.05.045

Reference yield: 85.0%

N',N''-bis(3-carboxy-1-oxopropanyl) 2-amino-N-arylbenzamidine (1015164-91-6) + cobalt(II) chloride hexahydrate → cobalt(II) (N',N''-bis(3-carboxy-1-oxopropanyl)-2-amino-N-arylbenzamidine) (1020031-77-9)

Guidance literature:

In methanol; MeOH soln. of ligand added to MeOH soln. of CoCl2*6H2O, stirred for 3 h; vol. reduced on water bath, ppt. washed with H2O and MeOH, air dried, ppt. redissolved in MeOH, left for wk; elem. anal.;

DOI:10.1016/j.saa.2007.05.045

upstream raw materials:

succinic acid anhydride

2-amino-N′-phenylbenzamidine

Downstream raw materials:

[Hg(N',N''-bis(3-carboxy-1-oxo-propanyl) 2 amino-N-arylbenzamidine)]*H₂O

[Cd(N',N''-bis(3-carboxy-1-oxo-propanyl) 2 amino-N-arylbenzamidine)]*H₂O

[Zn(N',N''-bis(3-carboxy-1-oxo-propanyl) 2 amino-N-arylbenzamidine)]

cobalt(II) (N',N''-bis(3-carboxy-1-oxopropanyl)-2-amino-N-arylbenzamidine)