diethyl cyclohex-1-enylsuccinate

Base Information

Chemical Name:diethyl cyclohex-1-enylsuccinate
CAS No.:71932-44-0
Molecular Formula:C₁₄H₂₂O₄
Molecular Weight:254.326
Hs Code.:

Synonyms:diethyl cyclohex-1-enylsuccinate

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Chemical Property of diethyl cyclohex-1-enylsuccinate

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Technology Process of diethyl cyclohex-1-enylsuccinate

There total 3 articles about diethyl cyclohex-1-enylsuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 123-25-1
succinic acid diethyl ester

: 71932-44-0
diethyl cyclohex-1-enylsuccinate

Guidance literature:: cyclohexanone; succinic acid diethyl ester; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 16h;

With sulfuric acid; In ethanol; at 80 ℃; for 18h;
DOI:10.1055/s-2005-917082

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 71932-44-0
diethyl cyclohex-1-enylsuccinate

Guidance literature:: cyclohexanone; With ethanol; sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere; Cooling with ice;

cyclohexanone; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

With sulfuric acid; In ethanol; at 0 ℃; for 13h; Reflux; Inert atmosphere;
DOI:10.1021/acs.joc.5b02241