C₃₃H₃₃N₅O₃

Base Information

Chemical Name:C₃₃H₃₃N₅O₃
CAS No.:942041-42-1
Molecular Formula:C₃₃H₃₃N₅O₃
Molecular Weight:547.657
Hs Code.:

C<sub>33</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₃₃H₃₃N₅O₃

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Chemical Property of C₃₃H₃₃N₅O₃

Chemical Property:

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Technology Process of C₃₃H₃₃N₅O₃

There total 21 articles about C₃₃H₃₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 161596-05-0
(1S,2R,3R,4R)-2,3-di-O-benzyl-4-benzyloxymethylcyclohex-5-ene-1,2,3-triol

: 942041-42-1
C₃₃H₃₃N₅O₃

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In 1,4-dioxane; at 20 ℃; for 24h;
DOI:10.1016/j.tetlet.2007.03.031

Reference yield:

: 942041-32-9
C₂₀H₂₆O₆

: 942041-42-1
C₃₃H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 13 steps

1.1: 91 percent / AcOH; water / tetrahydrofuran / 1 h / 50 °C

2.1: 89 percent / NaH / dimethylformamide / 1 h / 20 °C

3.1: BH₃*Me₃S; NaOH; H₂O₂ / tetrahydrofuran / 24 h

3.2: oxalyl chloride; DMSO / CH₂Cl₂ / 4 h / -78 °C

4.1: 94 percent / Et₃N / CH₂Cl₂ / 168 h / 20 °C

5.1: 92 percent / NaBH₄ / ethanol; tetrahydrofuran / 0.17 h / 0 °C

6.1: 78 percent / NaH / dimethylformamide / 1 h / 20 °C

7.1: 66 percent / Cu(OTf)2; BH₃*THF / 1 h

8.1: 86 percent / PPh₃; I₂; imidazole / toluene / 3 h / Heating

9.1: 60 percent / DBU / tetrahydrofuran / Heating

10.1: 93 percent / HgCl₂ / acetone; H₂O / 1 h / Heating

11.1: 53 percent / MsCl; DAMP / pyridine / 24 h / 20 °C

12.1: NaBH₄; CeCl₃*7H₂O / ethanol; tetrahydrofuran / 0.17 h / -78 °C

13.1: 37 percent / Ph₃P; DIAD / dioxane / 24 h / 20 °C

With 1H-imidazole; sodium hydroxide; sodium tetrahydroborate; cerium(III) chloride; borane-THF; di-isopropyl azodicarboxylate; bisacodyl; water; dihydrogen peroxide; iodine; copper(II) bis(trifluoromethanesulfonate); sodium hydride; acetic acid; methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; mercury dichloride; In tetrahydrofuran; 1,4-dioxane; pyridine; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 10.1: Ferrier rearrangement / 13.1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2007.03.031

Reference yield:

: 3162-96-7
methyl 4,6-O-benzylidene-α-D-glucopyranoside

: 942041-42-1
C₃₃H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 18 steps

1.1: Bu₂SnO / toluene; methanol / 14 h / 55 °C

1.2: Et₃N / dioxane / 4 h / 20 °C

2.1: 95 percent / P-TsOH / CH₂Cl₂ / 1 h / 20 °C

3.1: 96 percent / NaOMe / methanol / 2 h / 20 °C

4.1: TFAA; DMSO; Et₃N / CH₂Cl₂ / -78 °C

5.1: n-BuLi / tetrahydrofuran / -78 °C

6.1: 91 percent / AcOH; water / tetrahydrofuran / 1 h / 50 °C

7.1: 89 percent / NaH / dimethylformamide / 1 h / 20 °C

8.1: BH₃*Me₃S; NaOH; H₂O₂ / tetrahydrofuran / 24 h

8.2: oxalyl chloride; DMSO / CH₂Cl₂ / 4 h / -78 °C

9.1: 94 percent / Et₃N / CH₂Cl₂ / 168 h / 20 °C

10.1: 92 percent / NaBH₄ / ethanol; tetrahydrofuran / 0.17 h / 0 °C

11.1: 78 percent / NaH / dimethylformamide / 1 h / 20 °C

12.1: 66 percent / Cu(OTf)2; BH₃*THF / 1 h

13.1: 86 percent / PPh₃; I₂; imidazole / toluene / 3 h / Heating

14.1: 60 percent / DBU / tetrahydrofuran / Heating

15.1: 93 percent / HgCl₂ / acetone; H₂O / 1 h / Heating

16.1: 53 percent / MsCl; DAMP / pyridine / 24 h / 20 °C

17.1: NaBH₄; CeCl₃*7H₂O / ethanol; tetrahydrofuran / 0.17 h / -78 °C

18.1: 37 percent / Ph₃P; DIAD / dioxane / 24 h / 20 °C

With 1H-imidazole; sodium hydroxide; sodium tetrahydroborate; n-butyllithium; cerium(III) chloride; borane-THF; di-isopropyl azodicarboxylate; bisacodyl; water; dihydrogen peroxide; iodine; sodium methylate; copper(II) bis(trifluoromethanesulfonate); sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; triphenylphosphine; trifluoroacetic anhydride; mercury dichloride; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; 5.1: Wittig reaction / 15.1: Ferrier rearrangement / 18.1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2007.03.031