2,3,4,5,6-pentamethylphenyl carbonochloridate

Base Information

Chemical Name:2,3,4,5,6-pentamethylphenyl carbonochloridate
CAS No.:284041-56-1
Molecular Formula:C₁₂H₁₅ClO₂
Molecular Weight:226.703
Hs Code.:

Synonyms:2,3,4,5,6-pentamethylphenyl carbonochloridate

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Chemical Property of 2,3,4,5,6-pentamethylphenyl carbonochloridate

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Technology Process of 2,3,4,5,6-pentamethylphenyl carbonochloridate

There total 2 articles about 2,3,4,5,6-pentamethylphenyl carbonochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-44-5
phosgene

: 2819-86-5
pentamethylphenol

: 284041-56-1
2,3,4,5,6-pentamethylphenyl carbonochloridate

Guidance literature:: With N,N-dimethyl-aniline; In toluene; at 0 - 20 ℃; for 18h;
DOI:10.1002/(SICI)1522-2675(20000510)83:5<1022::AID-HLCA1022>3.0.CO;2-Y

Reference yield:

: 194211-77-3
3,5-bis(bromomethyl)-2,4,6-trimethylphenol

: 284041-56-1
2,3,4,5,6-pentamethylphenyl carbonochloridate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂; conc. aq. AcONa / 10 percent Pd/C / ethyl acetate; ethanol; acetic acid / 20 °C

2: 95 percent / N,N-dimethylaniline / toluene / 18 h / 0 - 20 °C

With hydrogen; sodium acetate; N,N-dimethyl-aniline; palladium on activated charcoal; In ethanol; acetic acid; ethyl acetate; toluene; 1: Hydrogenation / 2: Acylation;
DOI:10.1002/(SICI)1522-2675(20000510)83:5<1022::AID-HLCA1022>3.0.CO;2-Y