C₄₁H₄₈O₁₆

Base Information

Chemical Name:C₄₁H₄₈O₁₆
CAS No.:306726-46-5
Molecular Formula:C₄₁H₄₈O₁₆
Molecular Weight:796.823
Hs Code.:

C<sub>41</sub>H<sub>48</sub>O<sub>16</sub>

Synonyms:C₄₁H₄₈O₁₆

Suppliers and Price of C₄₁H₄₈O₁₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₄₁H₄₈O₁₆

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₄₁H₄₈O₁₆

There total 44 articles about C₄₁H₄₈O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 32315-10-9
bis(trichloromethyl) carbonate

: 306726-45-4
C₄₀H₅₀O₁₅

: 306726-46-5
C₄₁H₄₈O₁₆

Guidance literature:: With pyridine; In dichloromethane; at -78 - 25 ℃; for 1h;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8

Reference yield:

: 256341-98-7
(3aR,4S,7R,7aS)-2,2-Dimethyl-4-phenylselanyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ol

: 306726-46-5
C₄₁H₄₈O₁₆

Guidance literature:: Multi-step reaction with 15 steps

1.1: NaH / dimethylformamide / 0.08 h / 0 °C

1.2: 95 percent / nBu₄NI / dimethylformamide / 2 h / 0 - 25 °C

2.1: 96 percent / PPTS; MeOH / 1 h / 25 °C

3.1: 91 percent / 2,6-lutidine / tetrahydrofuran / 0.5 h / -78 °C

4.1: 100 percent / DAST / CH₂Cl₂ / 0.5 h / 0 °C

5.1: 92 percent / SnCl₂ / diethyl ether / 3 h / 0 - 25 °C

6.1: 98 percent / K₂CO₃; MeOH / diethyl ether / 1 h / 25 °C

7.1: aq. NaIO₄; NaHCO₃ / methanol; CH₂Cl₂ / 2 h / 25 °C

8.1: 430 mg / iPr₂NH; vinyl acetate / toluene / 12 h / 140 °C

9.1: 95 percent / TBAF / tetrahydrofuran / 0.5 h / 0 °C

10.1: 97 percent / Et₃N; DMAP / CH₂Cl₂ / 2 h / 0 - 25 °C

11.1: 95 percent / TBAF; AcOH / tetrahydrofuran / 1 h / 25 °C

12.1: 85 percent / Martin sulfurane; Et₃N / CHCl₃ / 2 h / 50 °C

13.1: NMO; H₂O; OsO₄ / quinuclidine / acetone; 2-methyl-propan-2-ol / 24 h / 25 °C

14.1: 98 percent / K₂CO₃; MeOH / 4 h / 25 °C

15.1: 96 percent / pyridine / CH₂Cl₂ / 1 h / -78 - 25 °C

With pyridine; 2,6-dimethylpyridine; methanol; dmap; sodium periodate; osmium(VIII) oxide; vinyl acetate; N-methyl-2-indolinone; Martins sulfurane; tetrabutyl ammonium fluoride; water; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; diisopropylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; tin(ll) chloride; Quinuclidine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol; 1.1: Metallation / 1.2: Etherification / 2.1: Ring cleavage / 3.1: Etherification / 4.1: Rearrangement / 5.1: Glycosidation / 6.1: Deacylation / 7.1: Oxidation / 8.1: Cyclization / 9.1: Silyl ether cleavage / 10.1: Esterification / 11.1: Silyl ether cleavage / 12.1: Dehydration / 13.1: Oxidation / 14.1: Debenzoylation / 15.1: Cyclization;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8

Reference yield:

: 256342-00-4
(2S,3R,4R,5R)-5-(4-Methoxy-benzyloxy)-2-phenylselanyl-tetrahydro-pyran-3,4-diol

: 306726-46-5
C₄₁H₄₈O₁₆

Guidance literature:: Multi-step reaction with 13 steps

1: 91 percent / 2,6-lutidine / tetrahydrofuran / 0.5 h / -78 °C

2: 100 percent / DAST / CH₂Cl₂ / 0.5 h / 0 °C

3: 92 percent / SnCl₂ / diethyl ether / 3 h / 0 - 25 °C

4: 98 percent / K₂CO₃; MeOH / diethyl ether / 1 h / 25 °C

5: aq. NaIO₄; NaHCO₃ / methanol; CH₂Cl₂ / 2 h / 25 °C

6: 430 mg / iPr₂NH; vinyl acetate / toluene / 12 h / 140 °C

7: 95 percent / TBAF / tetrahydrofuran / 0.5 h / 0 °C

8: 97 percent / Et₃N; DMAP / CH₂Cl₂ / 2 h / 0 - 25 °C

9: 95 percent / TBAF; AcOH / tetrahydrofuran / 1 h / 25 °C

10: 85 percent / Martin sulfurane; Et₃N / CHCl₃ / 2 h / 50 °C

11: NMO; H₂O; OsO₄ / quinuclidine / acetone; 2-methyl-propan-2-ol / 24 h / 25 °C

12: 98 percent / K₂CO₃; MeOH / 4 h / 25 °C

13: 96 percent / pyridine / CH₂Cl₂ / 1 h / -78 - 25 °C

With pyridine; 2,6-dimethylpyridine; methanol; dmap; sodium periodate; osmium(VIII) oxide; vinyl acetate; N-methyl-2-indolinone; Martins sulfurane; tetrabutyl ammonium fluoride; water; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; diisopropylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; tin(ll) chloride; Quinuclidine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; acetone; toluene; tert-butyl alcohol; 1: Etherification / 2: Rearrangement / 3: Glycosidation / 4: Deacylation / 5: Oxidation / 6: Cyclization / 7: Silyl ether cleavage / 8: Esterification / 9: Silyl ether cleavage / 10: Dehydration / 11: Oxidation / 12: Debenzoylation / 13: Cyclization;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8