(S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid

Base Information

• Chemical Name: (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid
• CAS No.: 1632042-08-0
• Molecular Formula: C₁₄H₁₉N₅O₅S
• Molecular Weight: 369.401

Synonyms:(S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid

Chemical Property of (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid

Chemical Property:

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Technology Process of (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid

There total 1 articles about (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Cbzα-L-ωNO2-Arg-Bt (1052265-47-0) → (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid (1632042-08-0)

Guidance literature:

With 4-methyl-morpholine; hydrogen sulfide; In tetrahydrofuran; at 0 - 20 ℃; for 1.08333h; Inert atmosphere;

DOI:10.1055/s-0033-1340292

Reference yield: 80.0%

propylamine (107-10-8,42939-71-9) + (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid (1632042-08-0) → benzyl-(S)-(5-(2-nitroguanidino)-1-oxo-1-(propylamino)pentan-2-yl)carbamate

Guidance literature:

With isopentyl nitrite; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Darkness;

DOI:10.1039/c4ra04897k

Reference yield: 78.0%

3-(1H-imidazol-1-yl)propan-1-amine (5036-48-6) + (S)-2-(((benzyloxy)carbonyl)amino)-5-(2-nitroguanidino)pentanethioic S-acid (1632042-08-0) → benzyl-(S)-(1-((3-(1H-imidazol-1-yl)propyl)amino)-5-(2-nitroguanidino)-1-oxopentan-2-yl)carbamate

Guidance literature:

With isopentyl nitrite; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Darkness;

DOI:10.1039/c4ra04897k

upstream raw materials:

Cbzα-L-ωNO2-Arg-Bt

Downstream raw materials:

methyl-N²-((benzyloxy)carbonyl)-N^ω'-nitro-L-arginyl-L-valinate

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