1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine

Base Information

• Chemical Name: 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine
• CAS No.: 214541-77-2
• Molecular Formula: C₂₈H₄₂N₆O₈Si₂
• Molecular Weight: 646.848

Synonyms:1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine

Chemical Property of 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine

There total 5 articles about 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-chloro-2,4-dinitro-benzene (97-00-7) + 3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine (106568-83-6) → 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine (214541-77-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2.5h;

DOI:10.1016/S0040-4039(98)01605-0

Reference yield:

2-deoxyinosine (890-38-0) → 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine (214541-77-2)

Guidance literature:

Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 16 h / Ambient temperature

2: 96 percent / K₂CO₃ / dimethylformamide / 2.5 h / 80 °C

With 1H-imidazole; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(98)01605-0

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → 1-N-(2,4-dinitrophenyl)-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine (214541-77-2)

Guidance literature:

Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 16 h / Ambient temperature

2: 96 percent / K₂CO₃ / dimethylformamide / 2.5 h / 80 °C

With 1H-imidazole; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(98)01605-0

upstream raw materials:

1-chloro-2,4-dinitro-benzene

3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyinosine

2-deoxyinosine

tert-butyldimethylsilyl chloride

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