C₁₇H₁₉N₃O₂

Base Information

• Chemical Name: C₁₇H₁₉N₃O₂
• CAS No.: 1413439-92-5
• Molecular Formula: C₁₇H₁₉N₃O₂
• Molecular Weight: 297.357
• Mol file: 1413439-92-5.mol

Synonyms:C₁₇H₁₉N₃O₂

Chemical Property of C₁₇H₁₉N₃O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₇H₁₉N₃O₂

There total 4 articles about C₁₇H₁₉N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C12H18N4O4S (1413439-89-0) + 4-methoxyphenyl magnesium bromide (13139-86-1) → C17H19N3O2 (1413439-92-5)

Guidance literature:

With chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II); In tetrahydrofuran; at 40 ℃;

DOI:10.1038/nchem.1504

Reference yield:

C17H24N2O4SSi (1413439-83-4) → C17H19N3O2 (1413439-92-5)

Guidance literature:

Multi-step reaction with 4 steps

1: hydrogen; palladium on activated charcoal / ethyl acetate

2: n-butyllithium / diethyl ether / -78 °C

3: cesium fluoride

4: chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II) / tetrahydrofuran / 40 °C

With n-butyllithium; chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II); palladium on activated charcoal; hydrogen; cesium fluoride; In tetrahydrofuran; diethyl ether; ethyl acetate;

DOI:10.1038/nchem.1504

Reference yield:

C10H18N2O4SSi (1413439-97-0) → C17H19N3O2 (1413439-92-5)

Guidance literature:

Multi-step reaction with 3 steps

1: n-butyllithium / diethyl ether / -78 °C

2: cesium fluoride

3: chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II) / tetrahydrofuran / 40 °C

With n-butyllithium; chloro(η⁵-cyclopentadienyl)(1,3-dimesitylimidazol-2-ylidene)nickel(II); cesium fluoride; In tetrahydrofuran; diethyl ether;

DOI:10.1038/nchem.1504

upstream raw materials:

C₁₇H₂₄N₂O₄SSi

C₁₀H₁₈N₂O₄SSi

C₁₁H₁₇F₃N₂O₆S₂Si

C₁₂H₁₈N₄O₄S