N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide

Base Information

• Chemical Name: N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide
• CAS No.: 1391708-38-5
• Molecular Formula: C₂₇H₂₂INO₃S
• Molecular Weight: 567.447
• Mol file: 1391708-38-5.mol

Synonyms:N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide

Chemical Property of N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide

Chemical Property:

Purity/Quality:

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Technology Process of N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide

There total 1 articles about N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-Iodobenzoyl chloride (609-67-6) + N-(2-allylnaphthalen-1-yl)-4-methylbenzenesulfonamide (56799-90-7) → N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide (1391708-38-5)

Guidance literature:

With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1055/s-0031-1290970

Reference yield: 61.0%

N-(2-allyl-1-naphthyl)-2-iodo-N-(p-tolylsulfonyl)benzamide (1391708-38-5) → 8-methylene-14-tosyl-7,14-dihydrobenzo[f]naphtho[1,2-b]azocin-13(8H)-one (1391708-45-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium acetate; In N,N-dimethyl-formamide; at 90 ℃; for 8h; regioselective reaction; Inert atmosphere;

DOI:10.1055/s-0031-1290970

upstream raw materials:

2-Iodobenzoyl chloride

N-(2-allylnaphthalen-1-yl)-4-methylbenzenesulfonamide

Downstream raw materials:

8-methylene-14-tosyl-7,14-dihydrobenzo[f]naphtho[1,2-b]azocin-13(8H)-one