3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

Base Information

Chemical Name:3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid
CAS No.:1428548-22-4
Molecular Formula:C₂₂H₂₀N₄O₅
Molecular Weight:420.425
Hs Code.:

Synonyms:3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

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Chemical Property of 3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

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Technology Process of 3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

There total 15 articles about 3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1428548-12-2
ethyl N-({5-[(diphenylmethyl)carbamoyl]-4-hydroxypyrimidin-2-yl}carbonyl)-β-alaninate

: 1428548-22-4
3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

Guidance literature:: With water; potassium hydroxide; at 50 ℃; for 0.5h;

Reference yield:

: tert-butyl 3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoate

: 1428548-22-4
3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 6h;

Reference yield:

: 1428548-42-8
N-benzhydryl-2-((benzyloxy)methyl)-4-hydroxypyrimidine-5-carboxamide

: 1428548-22-4
3-(5-(benzhydrylcarbamoyl)-4-hydroxypyrimidine-2-carboxamido)propanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: palladium on activated charcoal; ammonium formate / methanol / Reflux

2: Dess-Martin periodane / dichloromethane / 20 °C

3: sodium chlorite; sodium hydrogenphosphate dodecahydrate / water; tert-butyl alcohol / 20 °C

4: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 20 °C

5: water; potassium hydroxide / 0.5 h / 50 °C

With sodium chlorite; sodium hydrogenphosphate dodecahydrate; palladium on activated charcoal; water; ammonium formate; Dess-Martin periodane; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In methanol; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;