Technology Process of methyl 2-propyl-3-oxo-3-phenylpropanoate
There total 5 articles about methyl 2-propyl-3-oxo-3-phenylpropanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylsilane; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
1,2-dichloro-ethane;
at 60 ℃;
for 10h;
DOI:10.1002/anie.200906349
- Guidance literature:
-
N-isopropylbenzamide;
With
2-fluoropyridine; trifluoromethylsulfonic anhydride;
In
dichloromethane;
at 0 ℃;
for 0.333333h;
Inert atmosphere;
Schlenk technique;
methyl 2-(pyrrolidin-1-ylmethylene)pentanoate;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
Schlenk technique;
With
hydrogenchloride;
In
dichloromethane; water;
at 20 ℃;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/adsc.201801443
- Guidance literature:
-
methyl 2-formylvalerate;
With
pyrrolidine;
In
dichloromethane;
at 0 - 20 ℃;
for 2h;
Inert atmosphere;
Schlenk technique;
Molecular sieve;
N-isopropylbenzamide;
With
2-fluoropyridine; trifluoromethylsulfonic anhydride;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
Schlenk technique;
Molecular sieve;
With
hydrogenchloride;
In
dichloromethane; water;
at 20 ℃;
Inert atmosphere;
Schlenk technique;
Molecular sieve;
DOI:10.1002/adsc.201801443
