6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

Base Information

Chemical Name:6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose
CAS No.:910222-11-6
Molecular Formula:C₁₆H₂₁N₃O₇S
Molecular Weight:399.425
Hs Code.:

Synonyms:6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

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Chemical Property of 6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

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Technology Process of 6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

There total 2 articles about 6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2484-55-1
2,3-O-isopropylidene-1,6-bis-O-(p-toluenesulfonyl)-α-L-sorbofuranose

: 910222-11-6
6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 75 ℃; for 30h;
DOI:10.1016/j.carres.2006.06.002

Reference yield:

: 17682-71-2
2,3-O-isopropylidene-α-L-sorbofuranose

: 910222-11-6
6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / pyridine / 5 h / 20 °C

2: 89 percent / NaN₃ / dimethylformamide / 30 h / 75 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2006.06.002

Reference yield:

: 910222-11-6
6-azido-6-deoxy-2,3-O-isopropylidene-1-O-(p-toluenesulfonyl)-α-L-sorbofuranose

: 1121-25-1,55780-69-3
2-methyl-3-pyridinol

Guidance literature:: Multi-step reaction with 2 steps

1: 40.3 percent / LiAlH₄ / tetrahydrofuran / 30 h / Heating

2: Dowex 50(H+); H₂ / Pd(OH)2/C / H₂O / 30 h / 3102.89 Torr / pH 3 - 4

With lithium aluminium tetrahydride; Dowex 50(H+); hydrogen; palladium dihydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.carres.2006.06.002