(-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide

Base Information

Chemical Name:(-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide
CAS No.:350479-89-9
Molecular Formula:C₂₄H₃₈N₃O₂PS
Molecular Weight:463.624
Hs Code.:

Synonyms:(-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide

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Chemical Property of (-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide

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Technology Process of (-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide

There total 2 articles about (-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3560-15-4
tetraethyldiamidophosphite

: 318471-67-9
(S)-(+)-N-α-methyl-(4-methylbenzylidene)-p-toluenesulfinamide

: 350479-89-9
(-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide

Guidance literature:: tetraethyldiamidophosphite; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 8h;

(S)-(+)-N-α-methyl-(4-methylbenzylidene)-p-toluenesulfinamide; In tetrahydrofuran; at -78 ℃; for 8h; Further stages.;
DOI:10.1021/ol015945f

Reference yield:

: 188447-91-8
(S)-p-toluenesulfinimide

: 350479-89-9
(-)-N,N-diethyl N-(p-toluenesulfinyl)-1-amino-1-(p-tolyl)ethylphosphamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Ti(OEt)4

2.1: LiHMDS / tetrahydrofuran / 8 h / -78 °C

2.2: 78 percent / tetrahydrofuran / 8 h / -78 °C

With titanium(IV) tetraethanolate; lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1021/ol015945f