2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

Base Information

Chemical Name:2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate
CAS No.:1255209-41-6
Molecular Formula:C₁₈H₂₂BNO₇
Molecular Weight:375.186
Hs Code.:

Synonyms:2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

Suppliers and Price of 2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of 2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

There total 3 articles about 2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 74124-79-1
di(succinimido) carbonate

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1255209-41-6
2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1039/c0cc01560a

Reference yield:

: 59016-93-2
p-hydroxymethylphenylboronic acid

: 1255209-41-6
2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With sodium sulfate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201811261

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1255209-41-6
2,5-dioxopyrrolidin-1-yl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere

With sodium sulfate; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201811261