N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine

Base Information

• Chemical Name: N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine
• CAS No.: 866768-64-1
• Molecular Formula: C₂₃H₂₅ClIN₅O₂
• Molecular Weight: 565.841

Synonyms:N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine

Chemical Property of N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine

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Technology Process of N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine

There total 1 articles about N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

6-chloro-N2-(3-chloro-4-methoxy-phenyl)-N4-cycloheptyl-[1,3,5]triazine-2,4-diamine (502767-50-2) + p-Iodophenol (540-38-5) → N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine (866768-64-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 12h;

Reference yield: 72.0%

N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine (866768-64-1) + 2-methyl-but-3-yn-2-ol (115-19-5) → 4-{4-[4-(3-Chloro-4-methoxy-phenylamino)-6-cycloheptylamino-[1,3,5]triazin-2-yloxy]-phenyl}-2-methyl-but-3-yn-2-ol (866768-66-3)

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In N,N-dimethyl-formamide; for 6h;

Reference yield: 66.0%

N-(3-Chloro-4-methoxy-phenyl)-N'-cycloheptyl-6-(4-iodo-phenoxy)-[1,3,5]triazine-2,4-diamine (866768-64-1) + ethyl acrylate (140-88-5,9003-32-1) → 3-{4-[4-(3-Chloro-4-methoxy-phenylamino)-6-cycloheptylamino-[1,3,5]triazin-2-yloxy]-phenyl}-acrylic acid ethyl ester

Guidance literature:

With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 80 ℃; for 3h;

upstream raw materials:

6-chloro-N₂-(3-chloro-4-methoxy-phenyl)-N₄-cycloheptyl-[1,3,5]triazine-2,4-diamine

p-Iodophenol

Downstream raw materials:

4-{4-[4-(3-Chloro-4-methoxy-phenylamino)-6-cycloheptylamino-[1,3,5]triazin-2-yloxy]-phenyl}-2-methyl-but-3-yn-2-ol

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