2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose
CAS No.:74293-20-2
Molecular Formula:C₅₅H₅₉NO₁₀
Molecular Weight:894.074
Hs Code.:

2,3,4,6-tetra-O-benzyl-1-O-<N-benzyloxycarbonyl-O-(tert-butyl)-L-tyrosyl>-β-D-glucopyranose

Synonyms:2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

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Chemical Property of 2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

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Technology Process of 2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

There total 2 articles about 2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5545-54-0
N-(benzyloxycarbonyl)-O-(1,1-dimethylethyl)-L-tyrosine

: 74293-20-2
2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / DCC / ethyl acetate

2: 214 mg / imidazole / CH₂Cl₂ / 24 h / Ambient temperature

With 1H-imidazole; dicyclohexyl-carbodiimide; In dichloromethane; ethyl acetate;
DOI:10.1016/S0008-6215(00)85315-X

Reference yield:

: 6564-72-3
2,3,4,6-tetra-O-benzyl-D-glucopyranose

: 74293-19-9
N-benzyloxycarbonyl-O-(tert-butyl)-L-tyrosine p-nitrophenyl ester

: 74293-20-2
2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

: 74293-21-3
2,3,4,6-tetra-O-benzyl-1-O--α-D-glucopyranose

Guidance literature:: With 1H-imidazole; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85315-X

Reference yield: 98.0%

: 74293-20-2
2,3,4,6-tetra-O-benzyl-1-O--β-D-glucopyranose

: 76-05-1
trifluoroacetic acid

: 74293-25-7
1-O-(L-tyrosyl)-β-D-glucopyranose trifluoroacetate salt

Guidance literature:: With hydrogen; palladium on activated charcoal; In 2-methoxy-ethanol; for 24h; under 760 Torr;
DOI:10.1016/S0008-6215(00)85315-X