Technology Process of C37H44O8
There total 20 articles about C37H44O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tert.-butylhydroperoxide; selenium(IV) oxide;
In
dichloromethane;
at 0 ℃;
DOI:10.1021/ja00206a050
- Guidance literature:
-
Multi-step reaction with 7 steps
1: MnO2 / CH2Cl2
2: H2 / Pt/C / ethyl acetate / 760 Torr
3: 1.) ArSeCN, (n-Bu)3P, 2.) m-CPBA / 1.) THF, room temp., 2.) CH2Cl2, -78 deg C
4: KCN / methanol
5: DMAP / CH2Cl2
6: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH2Cl2
7: 50 percent / SeO2, t-BuOOH / CH2Cl2 / 0 °C
With
tert.-butylhydroperoxide; dmap; potassium cyanide; manganese(IV) oxide; selenium(IV) oxide; tributylphosphine; hydrogen; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid;
platinum on activated charcoal;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00206a050
- Guidance literature:
-
Multi-step reaction with 6 steps
1: H2 / Pt/C / ethyl acetate / 760 Torr
2: 1.) ArSeCN, (n-Bu)3P, 2.) m-CPBA / 1.) THF, room temp., 2.) CH2Cl2, -78 deg C
3: KCN / methanol
4: DMAP / CH2Cl2
5: 1.) DIBAH, 2.) DMAP / 1.) toluene, 2.) pyridine, CH2Cl2
6: 50 percent / SeO2, t-BuOOH / CH2Cl2 / 0 °C
With
tert.-butylhydroperoxide; dmap; potassium cyanide; selenium(IV) oxide; tributylphosphine; hydrogen; diisobutylaluminium hydride; 3-chloro-benzenecarboperoxoic acid;
platinum on activated charcoal;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja00206a050
