(2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Base Information

• Chemical Name: (2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine
• CAS No.: 197524-51-9
• Molecular Formula: C₁₄H₁₁N₅O₂
• Molecular Weight: 281.274
• Mol file: 197524-51-9.mol

Synonyms:(2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Chemical Property of (2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine

There total 1 articles about (2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-azidobenzylamine (96308-13-3) + 4-nitrobenzaldehdye (555-16-8) → (2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine (197524-51-9)

Guidance literature:

With magnesium sulfate; In diethyl ether; for 12h; Ambient temperature;

DOI:10.1016/S0040-4039(96)02054-0

Reference yield:

(2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine (197524-51-9) → 4-nitrobenzaldehdye (555-16-8)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 0.5 h / 20 °C

2: phenacetyl chloride; Et₃N

With triethylamine; phenylacetyl chloride; In toluene; 1: Substitution / 2: Cyclization;

DOI:10.1016/S0040-4020(97)00855-7

Reference yield:

diphenyl ketene (525-06-4) + (2-Azido-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine (197524-51-9) → 1-(2-Azido-benzyl)-4-(4-nitro-phenyl)-3,3-diphenyl-azetidin-2-one

Guidance literature:

In toluene; for 1h; Ambient temperature;

DOI:10.1055/s-1998-1920

upstream raw materials:

2-azidobenzylamine

4-nitrobenzaldehdye

Downstream raw materials:

4-nitrobenzaldehdye

2-(4-nitrophenyl)-1,2,3,4-tetrahydroquinazoline

2,2-diphenyl-1-(4-nitrophenyl)-1,2-dihydroazeto[2,1-b]quinazoline

(2-Azido-5-methyl-benzyl)-[1-(4-nitro-phenyl)-meth-(E)-ylidene]-amine