methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

Base Information

Chemical Name:methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate
CAS No.:1082204-13-4
Molecular Formula:C₂₅H₃₀BNO₆
Molecular Weight:451.327
Hs Code.:

Synonyms:methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

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Chemical Property of methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

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Technology Process of methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

There total 2 articles about methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1082204-11-2
methyl 1-benzyl-3-bromo-5,6-dimethoxy-1H-indole-2-carboxylate

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1082204-15-6
C₁₉H₁₉NO₄

: 1082204-13-4
methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triethylamine; XPhos; In 1,4-dioxane; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1021/jo801846b

Reference yield:

: 1082204-11-2
methyl 1-benzyl-3-bromo-5,6-dimethoxy-1H-indole-2-carboxylate

: 73183-34-3
bis(pinacol)diborane

: 1082204-15-6
C₁₉H₁₉NO₄

: 1082204-13-4
methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; at 110 ℃; for 14h; Inert atmosphere;
DOI:10.1021/jo801846b

Reference yield: 85.0%

: 1082204-19-0
methyl 1-benzyl-4-bromo-5,6-dimethoxy-1H-indole-2-carboxylate

: 1082204-13-4
methyl 1-benzyl-5,6-dimethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-indole-2-carboxylate

: 1082204-22-5
methyl 3-(2-(methoxycarbonyl)-1-benzyl-5,6-dimethoxy-1H-indol-4-yl)-1-benzyl-5,6-dimethoxy-1H-indole-2-carboxylate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium phosphate monohydrate; XPhos; In 1,4-dioxane; water; at 100 ℃; for 14h; Inert atmosphere;
DOI:10.1021/jo801846b