bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

Base Information

Chemical Name:bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide
CAS No.:1591653-36-9
Molecular Formula:C₂₈H₄₅O₁₀P
Molecular Weight:572.633
Hs Code.:

Synonyms:bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

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Chemical Property of bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

Chemical Property:

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Technology Process of bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

There total 3 articles about bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₄₅O₉P

: 1591653-36-9
bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

Guidance literature:: With dihydrogen peroxide; In toluene; at 0 ℃; for 1.5h;

Reference yield:

: C₁₀H₁₂OP^(1-)*Na⁽¹⁺⁾

: 1591653-36-9
bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / diethyl ether / 0.5 h / 0 °C

1.2: 1.5 h / 0 - 20 °C

2.1: dihydrogen peroxide / toluene / 1.5 h / 0 °C

With hydrogenchloride; dihydrogen peroxide; In diethyl ether; toluene;

Reference yield:

: 1754-55-8
ethyl 2,4,6-trimethylbenzoate

: 1591653-36-9
bis-3-[2-(2-ethoxyethoxy)ethoxycarbonyl]ethyl(2,4,6-trimethylbenzoy)phosphine oxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium; phosphorus; naphthalene; tert-butyl alcohol / 1,2-dimethoxyethane / 16 h / 60 °C

2.1: hydrogenchloride / diethyl ether / 0.5 h / 0 °C

2.2: 1.5 h / 0 - 20 °C

3.1: dihydrogen peroxide / toluene / 1.5 h / 0 °C

With hydrogenchloride; naphthalene; phosphorus; dihydrogen peroxide; sodium; tert-butyl alcohol; In 1,2-dimethoxyethane; diethyl ether; toluene;