4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

Base Information

Chemical Name:4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid
CAS No.:1352916-22-3
Molecular Formula:C₄₁H₅₇F₃N₂O₂
Molecular Weight:666.911
Hs Code.:

Synonyms:4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

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Chemical Property of 4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

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Technology Process of 4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

There total 3 articles about 4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.9%

: 30459-17-7
1-[4-(trifluoromethyl)phenyl]piperazine

: 150841-01-3
betulonic acid chloride

: 1352916-22-3
4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 48h; Inert atmosphere;
DOI:10.1007/s10600-011-0051-x

Reference yield:

: 473-98-3
betulin

: 1352916-22-3
4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent

2: oxalyl dichloride / dichloromethane

3: triethylamine / dichloromethane / 48 h / 25 °C / Inert atmosphere

With Jones reagent; oxalyl dichloride; triethylamine; In dichloromethane;
DOI:10.1007/s10600-011-0051-x

Reference yield:

: 4481-62-3
betulonic acid

: 1352916-22-3
4-(4′-trifluoromethylphenylpiperazine-1-yl) amide of betulonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane

2: triethylamine / dichloromethane / 48 h / 25 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; In dichloromethane;
DOI:10.1007/s10600-011-0051-x