4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

Base Information

Chemical Name:4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline
CAS No.:83789-94-0
Molecular Formula:C₁₈H₂₄N₂O₄
Molecular Weight:332.4
Hs Code.:

Synonyms:4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

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Chemical Property of 4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

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Technology Process of 4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

There total 11 articles about 4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₂₂H₂₈N₂O₆

: 83789-94-0
4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

Guidance literature:: With hydrogenchloride; In ethanol; for 15h; Reflux;
DOI:10.1080/10610278.2019.1578884

Reference yield: 81.0%

: 83841-01-4
triethyleneglycol bis(p-nitrophenyl)ether

: 83789-94-0
4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

Guidance literature:: With 10% palladium on activated charcoal; hydrazine hydrate;
DOI:10.5012/jkcs.2010.54.5.659

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 83789-94-0
4,4'-(2,2'-(ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy)dianiline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 8 h / Inert atmosphere; Reflux

2: hydrazine hydrate; palladium 10% on activated carbon / methanol / 10 h / Reflux

With palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; In methanol; acetonitrile;
DOI:10.1039/c6cc03144g