2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

Base Information

Chemical Name:2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate
CAS No.:1219687-55-4
Molecular Formula:C₂₇H₂₇NO₆
Molecular Weight:461.514
Hs Code.:

Synonyms:2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

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Chemical Property of 2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

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Technology Process of 2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

There total 5 articles about 2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240163-16-9
(1R,3S)-2-(benzyloxycarbonyl)-6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

: 1219687-55-4
2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

Guidance literature:: With potassium hydrogencarbonate; In acetone; Reflux;
DOI:10.1016/j.ejmech.2013.05.048

Reference yield:

: C₂₄H₂₁NO₆

: 77-78-1
dimethyl sulfate

: 1219687-55-4
2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

Guidance literature:: With potassium hydrogencarbonate; In acetone; for 16h; Reflux;
DOI:10.1002/ejoc.200901159

Reference yield:

: trans-1-phenyl-6,7-dihydroxy-1,2,3,4-tetrahydroisoquinoline-3-carboxylic acid

: 1219687-55-4
2-benzyl 3-methyl (1R,3S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2,3(1H)-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogencarbonate / 1,4-dioxane; water

2: potassium hydrogencarbonate / acetone / Reflux

With potassium hydrogencarbonate; In 1,4-dioxane; water; acetone;
DOI:10.1016/j.tetasy.2010.11.010