Technology Process of C18H21NO2S
There total 4 articles about C18H21NO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Methyltriphenylphosphonium bromide;
With
potassium tert-butylate;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
N-(2-(3-oxobutyl)phenyl)-4-methylbenzenesulfonamide;
In
tetrahydrofuran;
at 20 ℃;
DOI:10.1002/anie.201310983
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium diacetate; tetrabutyl-ammonium chloride; sodium carbonate / N,N-dimethyl-formamide / 48 h / 80 °C
2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C
2.2: 20 °C
With
potassium tert-butylate; tetrabutyl-ammonium chloride; palladium diacetate; sodium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
1.1: |Heck Reaction;
DOI:10.1002/anie.201310983
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / 1.5 h / 20 °C
2.1: palladium diacetate; tetrabutyl-ammonium chloride; sodium carbonate / N,N-dimethyl-formamide / 48 h / 80 °C
3.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C
3.2: 20 °C
With
pyridine; potassium tert-butylate; tetrabutyl-ammonium chloride; palladium diacetate; sodium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2.1: |Heck Reaction;
DOI:10.1002/anie.201310983