benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside
CAS No.:115973-77-8
Molecular Formula:C₂₉H₃₉FN₂O₁₃
Molecular Weight:642.633
Hs Code.:

Synonyms:benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Suppliers and Price of benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

There total 5 articles about benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 3554-95-8
benzyl 2-acetamido-3-O-acetyl-2-deoxy-α-D-galactopyranoside

: 115973-76-7,120664-91-7
2-methyl-(3,6-di-O-acetyl-1,2,4-trideoxy-4-fluoro-α-D-glucopyrano)-<2,1-d>-2-oxazoline

: 115973-77-8
benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 75 ℃; for 24h;
DOI:10.1016/0008-6215(88)80166-6

Reference yield:

: 75869-83-9
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranoside

: 115973-77-8
benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / diethylaminosulfur trifluoride / bis-(2-methoxy-ethyl) ether / 1 h / Ambient temperature

2: H₂ / 10percent Pd-C / acetic acid / 48 h / 2587.7 Torr / Ambient temperature

3: pyridine / 24 h / Ambient temperature

4: 69 percent / trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 24 h / 50 °C

5: 61 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 24 h / 75 °C

With diethylamino-sulfur trifluoride; trimethylsilyl trifluoromethanesulfonate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In pyridine; diethylene glycol dimethyl ether; acetic acid; 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(88)80166-6

Reference yield:

: 115973-74-5
benzyl 2-acetamido-3,6-di-O-benzyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside

: 115973-77-8
benzyl 2-acetamido-6-O-(2-acetamido-3,6-di-O-acetyl-2,4-dideoxy-4-fluoro-β-D-glucopyranosyl)-3-O-acetyl-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd-C / acetic acid / 48 h / 2587.7 Torr / Ambient temperature

2: pyridine / 24 h / Ambient temperature

3: 69 percent / trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 24 h / 50 °C

4: 61 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 24 h / 75 °C

With trimethylsilyl trifluoromethanesulfonate; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In pyridine; acetic acid; 1,2-dichloro-ethane;
DOI:10.1016/0008-6215(88)80166-6