Technology Process of Methyl-3--4-nitrobenzoat
There total 1 articles about Methyl-3--4-nitrobenzoat which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyrrolidine;
In
N,N-dimethyl-formamide;
for 4h;
Heating;
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
toluene;
for 6h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent / H2 / 5percent Pd/C / toluene / 6 h
2: 1.) AlCl3 / 1.) CH2Cl2, room temperature, 1 h, 2.) 3 h
3: 68 percent / NaBH4, BF3*OEt2 / tetrahydrofuran / 0.5 h
4: 66 percent / NEt3 / 3 h / Heating
With
sodium tetrahydroborate; aluminium trichloride; boron trifluoride diethyl etherate; hydrogen; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; toluene;