Methyl-3--4-nitrobenzoat

Base Information

Chemical Name:Methyl-3--4-nitrobenzoat
CAS No.:99474-17-6
Molecular Formula:C₁₁H₁₂N₂O₄
Molecular Weight:236.227
Hs Code.:

Methyl-3-<trans-2-(dimethylamino)vinyl>-4-nitrobenzoat

Synonyms:Methyl-3--4-nitrobenzoat

Suppliers and Price of Methyl-3--4-nitrobenzoat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-3--4-nitrobenzoat

Chemical Property:

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Technology Process of Methyl-3--4-nitrobenzoat

There total 1 articles about Methyl-3--4-nitrobenzoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3113-71-1
3-methyl-4-nitrobenzoic acid

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 99474-17-6
Methyl-3--4-nitrobenzoat

Guidance literature:: With pyrrolidine; In N,N-dimethyl-formamide; for 4h; Heating;

Reference yield: 75.0%

: 99474-17-6
Methyl-3--4-nitrobenzoat

: 1011-65-0
5-methoxycarbonylindole

Guidance literature:: With hydrogen; palladium on activated charcoal; In toluene; for 6h;

Reference yield:

: 99474-17-6
Methyl-3--4-nitrobenzoat

: 98323-99-0
Methyl-3-<4-(1,2,3,6-tetrahydro-4-phenyl-1-pyridyl)butyl>-5-indolcarboxylat

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / H₂ / 5percent Pd/C / toluene / 6 h

2: 1.) AlCl₃ / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 3 h

3: 68 percent / NaBH₄, BF₃*OEt₂ / tetrahydrofuran / 0.5 h

4: 66 percent / NEt₃ / 3 h / Heating

With sodium tetrahydroborate; aluminium trichloride; boron trifluoride diethyl etherate; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; toluene;