Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane]

Base Information

Chemical Name:Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane]
CAS No.:73057-70-2
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:
NSC Number:167983
DSSTox Substance ID:DTXSID70304885
Mol file:73057-70-2.mol

Synonyms:73057-70-2;Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane];spiro[1,3-dioxolane-2,6'-bicyclo[3.2.0]hept-2-ene];NSC167983;SCHEMBL23080551;DTXSID70304885;SAXYAQZQIDZGAF-UHFFFAOYSA-N;NSC-167983

Suppliers and Price of Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane]

Chemical Property:

Boiling Point:228.6oC at 760 mmHg
Flash Point:91.5oC
PSA：18.46000
Density:1.18g/cm3
LogP:1.32550
XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:152.083729621
Heavy Atom Count:11
Complexity:204

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC2(O1)CC3C2CC=C3

Technology Process of Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane]

There total 2 articles about Spiro[bicyclo[3.2.0]hept-2-ene-6,2'-[1,3]dioxolane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 13173-09-6,62182-73-4,71155-04-9,71155-05-0
bicyclo[3.2.0]hept-2-en-6-one

: 107-21-1
ethylene glycol

: 73057-70-2
cis-bicyclo<3.2.0>hept-2-en-6-one ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 73057-70-2
cis-bicyclo<3.2.0>hept-2-en-6-one ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Zn, AcOH

2: 90 percent / p-TsOH / benzene / Heating

With toluene-4-sulfonic acid; acetic acid; zinc; In benzene;