2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile

Base Information

• Chemical Name: 2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile
• CAS No.: 120512-11-0
• Molecular Formula: C₁₄H₁₆N₄O
• Molecular Weight: 256.307

Synonyms:2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile

Chemical Property of 2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile

Chemical Property:

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Technology Process of 2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile

There total 2 articles about 2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

3-(cyano-dimethyl-methyl)-5-[1,2,4]triazol-1-ylmethyl-benzoic acid methyl ester → 2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile (120512-11-0)

Guidance literature:

With sodium tetrahydroborate; polyethylene glycol 400; at 80 ℃; for 16h;

DOI:10.1039/b707768h

Reference yield:

→ 2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile (120512-11-0)

Guidance literature:

Reference yield: 82.0%

2-(3-hydroxymethyl-5-[1,2,4]triazol-1-ylmethylphenyl)-2-methylpropionitrile (120512-11-0) + 4-Benzyloxyphenol (103-16-2) → 2-(3-[(1H-1,2,4-triazol-1-yl)methyl]-5-{[4-(benzyloxy)phenoxy]methyl}phenyl)-2-methylpropanenitrile

Guidance literature:

With triphenylphosphine polystyrene; diethylazodicarboxylate; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/b707768h

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