(R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

Base Information

Chemical Name:(R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine
CAS No.:183017-91-6
Molecular Formula:C₄₄H₅₆N₂O₄S₂
Molecular Weight:741.072
Hs Code.:

Synonyms:(R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

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Chemical Property of (R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

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Technology Process of (R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

There total 6 articles about (R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 183017-87-0
(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

: 60-24-2
2-hydroxyethanethiol

: 183017-91-6
(R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In chloroform; at 80 ℃; for 20h;
DOI:10.1016/0957-4166(96)00284-4

Reference yield:

: 24623-65-2
3-tert-butyl-2-hydroxybenzaldehyde

: 183017-91-6
(R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / aq. HCl / 48 h / Ambient temperature

2: 90 percent / benzene / 1 h / Heating

3: 57 percent / aq. NaOH / 2 h / Ambient temperature

4: 96 percent / ethanol / 0.5 h

5: 81 percent / AIBN / CHCl₃ / 20 h / 80 °C

With hydrogenchloride; sodium hydroxide; 2,2'-azobis(isobutyronitrile); In ethanol; chloroform; benzene;
DOI:10.1016/0957-4166(96)00284-4

Reference yield:

: 35132-20-8
(R,R)-1,2-diphenylethylenediamine

: 183017-91-6
(R,R)-N,N'-bis[3-tert-butyl-5-[2-(hydroxyethylthio)ethyl]salicylidene]-1,2-diphenyl-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / ethanol / 0.5 h

2: 81 percent / AIBN / CHCl₃ / 20 h / 80 °C

With 2,2'-azobis(isobutyronitrile); In ethanol; chloroform;
DOI:10.1016/0957-4166(96)00284-4