(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

Base Information

Chemical Name:(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine
CAS No.:183017-87-0
Molecular Formula:C₄₀H₄₄N₂O₂
Molecular Weight:584.802
Hs Code.:

Synonyms:(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

Chemical Property:

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Technology Process of (R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

There total 4 articles about (R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 35132-20-8
(R,R)-1,2-diphenylethylenediamine

: 178159-74-5
3-tert-butyl-2-hydroxy-5-vinylbenzaldehyde

: 183017-87-0
(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

Guidance literature:: In ethanol; for 0.5h;
DOI:10.1016/0957-4166(96)00284-4

Reference yield:

: 24623-65-2
3-tert-butyl-2-hydroxybenzaldehyde

: 183017-87-0
(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / aq. HCl / 48 h / Ambient temperature

2: 90 percent / benzene / 1 h / Heating

3: 57 percent / aq. NaOH / 2 h / Ambient temperature

4: 96 percent / ethanol / 0.5 h

With hydrogenchloride; sodium hydroxide; In ethanol; benzene;
DOI:10.1016/0957-4166(96)00284-4

Reference yield:

: 183017-88-1
3-tert-butyl-5-(chloromethyl)-2-hydroxybenzaldehyde

: 183017-87-0
(R,R)-N,N'-bis(3-tert-butyl-5-vinylsalicylidene)-1,2-diphenyl-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / benzene / 1 h / Heating

2: 57 percent / aq. NaOH / 2 h / Ambient temperature

3: 96 percent / ethanol / 0.5 h

With sodium hydroxide; In ethanol; benzene;
DOI:10.1016/0957-4166(96)00284-4