methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

Base Information

Chemical Name:methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate
CAS No.:1558032-18-0
Molecular Formula:C₂₁H₂₂F₃NO₃
Molecular Weight:393.406
Hs Code.:

Synonyms:methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

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Chemical Property of methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

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Technology Process of methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

There total 2 articles about methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1558031-97-2
methyl (2E)-3-[(4S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl]prop-2-enoate

: 74467-05-3
N-hydroxy-4-(trifluoromethyl)benzenecarboximidoyl chloride

: 1558032-01-1
methyl (2E)-3-[(4S)-4-(2-methoxypropan-2-yl)cyclohex-1-en-1-yl]prop-2-enoate

: 1558032-18-0
methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

: C₂₁H₂₂F₃NO₃

: 1558032-16-8
methyl (2E)-3-[(4S)-4-{(5S)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

Guidance literature:: With Amberlyst-21; In dichloromethane; at 20 ℃; Overall yield = 96 %; regioselective reaction;
DOI:10.1016/j.molstruc.2013.12.035

Reference yield:

: 1558031-97-2
methyl (2E)-3-[(4S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl]prop-2-enoate

: 158611-70-2
(4-trifluoromethyl)phenyl nitrile oxide

: 1558032-01-1
methyl (2E)-3-[(4S)-4-(2-methoxypropan-2-yl)cyclohex-1-en-1-yl]prop-2-enoate

: 1558032-18-0
methyl (2E)-3-[(4S)-4-{(5R)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

: C₂₁H₂₂F₃NO₃

: 1558032-16-8
methyl (2E)-3-[(4S)-4-{(5S)-5-methyl-3-[4-(trifluoromethyl)phenyl]-4,5-dihydro-1,2-oxazol-5-yl}cyclohex-1-en-1-yl]prop-2-enoate

Guidance literature:: With methyl 4,6-O-benzylidene-α-D-glucopyranoside; ytterbium(III) triflate; In dichloromethane; Overall yield = 93 %; regioselective reaction;
DOI:10.1016/j.molstruc.2013.12.035