4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

Base Information

Chemical Name:4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide
CAS No.:1309763-80-1
Molecular Formula:C₂₀H₁₈N₆O
Molecular Weight:358.403
Hs Code.:

Synonyms:4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

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Chemical Property of 4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

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Technology Process of 4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

There total 4 articles about 4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1309763-77-6
4'-azido-2,2'-bipyridine-N'-oxide

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 1309763-80-1
4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1039/c1cc13683f

Reference yield:

: 33421-43-1
2,2'-bipyridyl N-oxide

: 1309763-80-1
4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 5 h / 100 °C

2: sodium azide / N,N-dimethyl-formamide / 48 h / 80 °C / Inert atmosphere

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 20 h / 20 °C / Inert atmosphere

With sodium azide; copper(ll) sulfate pentahydrate; sulfuric acid; nitric acid; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13683f

Reference yield:

: 14163-00-9
4-nitro-2,2'-bipyridine N-oxide

: 1309763-80-1
4'-(4-(4-(dimethylamino)phenyl)-1H-1,2,3-triazol-1-yl)-2,2'-bipyridine-N'-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 48 h / 80 °C / Inert atmosphere

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 20 h / 20 °C / Inert atmosphere

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c1cc13683f