6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

Base Information

Chemical Name:6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline
CAS No.:913331-56-3
Molecular Formula:C₂₂H₁₃ClF₃N
Molecular Weight:383.8
Hs Code.:

Synonyms:6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

Chemical Property:

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Technology Process of 6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

There total 2 articles about 6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1737-26-4
1-(4-trifluorophenyl)ethanol

: 719-59-5
5-chloro-2-aminobenzophenone

: 913331-56-3
6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

Guidance literature:: With benzophenone; dichlorotetrakis(dimethyl sulfoxide)ruthenium(II); potassium tert-butylate; at 100 ℃; for 48h;
DOI:10.1002/ejoc.200600945

Reference yield: 90.0%

: 709-63-7
1-(4-trifluoromethylphenyl)ethanone

: 719-59-5
5-chloro-2-aminobenzophenone

: 913331-56-3
6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

Guidance literature:: With sulfuric acid; acetic acid; at 80 ℃; for 2h;
DOI:10.24820/ark.5550190.p011.499

Reference yield: 60.0%

: 913331-56-3
6-chloro-2-[4-(trifluoromethyl)phenyl]-4-phenylquinoline

: iridium(III) chloride trihydrate

: 123-54-6,81235-32-7
acetylacetone

: 913331-24-5
Ir(acetylacetonato)(6-chloro-2-(4-trifluoromethylphenyl)-4-phenylquinoline(-1H))2

Guidance literature:: With Na₂CO₃; In 2-ethoxy-ethanol; water; under Ar; ligand and IrCl3*3H2O in EtOC2H4OH-H2O stirred (120°C, 24 h); cooled to room temp.; filtered; ppt. washed (H2O, EtOH, hexane); dried in vac.; mixed with acetylacetone and Na2CO3; dissolved in EtOC2H4OH; stirred (100°C, 16 h); cooled to room temp.; filtered; ppt. washed with H2O, EtOH and hexane; flash chromd. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1016/j.jorganchem.2006.07.008