4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

Base Information

Chemical Name:4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene
CAS No.:1427772-65-3
Molecular Formula:C₄₀H₅₆N₂OSi₂
Molecular Weight:637.068
Hs Code.:

Synonyms:4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

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Chemical Property of 4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

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Technology Process of 4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

There total 3 articles about 4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427772-61-9
4-dodecyloxy-3,5-diformylphenylacetylene

: 57792-17-3
2-aminophenyl-trimethylsilane

: 1427772-65-3
4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

Guidance literature:: With aluminum oxide; In toluene; at 20 ℃; for 18h;
DOI:10.1016/j.polymer.2013.02.009

Reference yield:

: 132431-13-1
N-(2-bromophenyl)-O-benzyl carbamate

: 1427772-65-3
4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C

1.2: 18 h / -78 - 20 °C

1.3: 24 h / 20 °C

2.1: aluminum oxide / toluene / 18 h / 20 °C

With aluminum oxide; n-butyllithium; In diethyl ether; hexane; toluene;
DOI:10.1016/j.polymer.2013.02.009

Reference yield:

: 548735-20-2
3,5-bis(hydroxymethyl)-4-dodecyloxy-1-phenylacetylene

: 1427772-65-3
4-dodecyloxy-3,5-bis(2-trimethylsilylphenyliminomethyl)phenylacetylene

Guidance literature:: Multi-step reaction with 2 steps

1: dipyridinium dichromate / dichloromethane / 48 h / 20 °C

2: aluminum oxide / toluene / 18 h / 20 °C

With aluminum oxide; dipyridinium dichromate; In dichloromethane; toluene;
DOI:10.1016/j.polymer.2013.02.009