C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

Base Information

Chemical Name:C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O
CAS No.:84666-32-0
Molecular Formula:C₂₂H₃₈OSn
Molecular Weight:437.253
Hs Code.:

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CH<sub>2</sub>C(Sn(C<sub>4</sub>H<sub>9</sub>)3)CH<sub>2</sub>O

Synonyms:C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

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Chemical Property of C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

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Technology Process of C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

There total 2 articles about C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 4039-82-1
Benzyl propargyl ether

: 688-73-3
tri-n-butyl-tin hydride

: 84666-32-0
C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

: 84666-31-9,109669-46-7,243662-95-5
<(1E)-3-(benzyloxy)-1-propen-1-yl>tributylstannate

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; hydrostannylation, at room temperature, mixture was stood for 10 minutes; removal of solvent (vacuo), flash chromy. (silica gel, dichloromethane);

Reference yield:

: 4039-82-1
Benzyl propargyl ether

: 688-73-3
tri-n-butyl-tin hydride

: 84666-32-0
C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

: 109669-46-7,84666-31-9,243662-95-5
<(1Z)-3-(benzyloxy)-1-propen-1-yl>tributylstannate

: 84666-31-9,109669-46-7,243662-95-5
<(1E)-3-(benzyloxy)-1-propen-1-yl>tributylstannate

Guidance literature:: With hydroquinone; tris(t-butyl isocyanide)tricarbonylmolybdenum(O); In tetrahydrofuran; alkyne dissolved in THF; catalyst and hydroquinone added; mixt warmed to60°C; Bu3SnH added; soln. stirred at 60°C for 12 h; solvent evapd. (vac.); purifn. by chromy. (eluent petrolether-EtOAc-NEt3);
DOI:10.1016/S0022-328X(01)01309-2

Reference yield: 93.0%

: 474009-16-0
3-(methoxymethoxy)-1-iodobenzene

: 84666-32-0
C₆H₅CH₂CH₂C(Sn(C₄H₉)3)CH₂O

: 1170721-77-3
C₁₈H₂₀O₃

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; lithium chloride; In N,N-dimethyl-formamide; at 90 ℃;
DOI:10.1016/j.tetlet.2009.03.069