2-methallyl-2-tolyl-2-MIDA boryl aldehyde

Base Information

• Chemical Name: 2-methallyl-2-tolyl-2-MIDA boryl aldehyde
• CAS No.: 1401572-31-3
• Molecular Formula: C₁₈H₂₂BNO₅
• Molecular Weight: 343.187
• Mol file: 1401572-31-3.mol

Synonyms:2-methallyl-2-tolyl-2-MIDA boryl aldehyde

Chemical Property of 2-methallyl-2-tolyl-2-MIDA boryl aldehyde

Chemical Property:

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Technology Process of 2-methallyl-2-tolyl-2-MIDA boryl aldehyde

There total 1 articles about 2-methallyl-2-tolyl-2-MIDA boryl aldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

N-methyliminodiacetyl (2-oxo-1-(p-tolyl)ethyl)boronate (1329422-56-1) + 3-hydroxy-2-methyl-1-propene (513-42-8) → 2-methallyl-2-tolyl-2-MIDA boryl aldehyde (1401572-31-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethyl borane; triethylamine; In tetrahydrofuran; at 50 ℃; for 48h; chemoselective reaction; Molecular sieve; Inert atmosphere; Sealed tube;

DOI:10.1039/c2ob26503f

upstream raw materials:

N-methyliminodiacetyl (2-oxo-1-(p-tolyl)ethyl)boronate

3-hydroxy-2-methyl-1-propene