2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Base Information

Chemical Name:2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate
CAS No.:69504-17-2
Molecular Formula:C₅₈H₈₂Cl₃N₄O₁₅PSi₃
Molecular Weight:1296.9
Hs Code.:

2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Synonyms:2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Suppliers and Price of 2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

There total 5 articles about 2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77245-03-5
C₅₈H₈₂Cl₃N₄O₁₄PSi₃

: 69504-17-2
2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Guidance literature:: With iodine; In tetrahydrofuran; water; for 0.0833333h; Ambient temperature;

Reference yield:

: Phosphorochloridous acid (2R,3R,4R,5R)-4-(tert-butyl-dimethyl-silanyloxy)-5-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester 2,2,2-trichloro-ethyl ester

: 69504-17-2
2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: collidine / tetrahydrofuran / 0.5 h / -78 °C

2: iodine / H₂O; tetrahydrofuran / 0.08 h / Ambient temperature

With 2,3,5-trimethyl-pyridine; iodine; In tetrahydrofuran; water;

Reference yield:

: 87418-87-9,69504-12-7
2',3'-bis-O-(tert-butyldimethylsilyl)uridine

: 69504-17-2
2,2,2-trichloroethyl 3'-[2'-O-(tert-butyldimethylsilyl)-5'-O-(p-methoxyphenyldiphenylmethyl)uridyl]-5'-[2',3'-O-(bis-tert-butyldimethylsilyl)uridyl] phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: collidine / tetrahydrofuran / 0.5 h / -78 °C

2: iodine / H₂O; tetrahydrofuran / 0.08 h / Ambient temperature

With 2,3,5-trimethyl-pyridine; iodine; In tetrahydrofuran; water;