2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

Base Information

Chemical Name:2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene
CAS No.:1286796-46-0
Molecular Formula:C₁₂H₁₅F
Molecular Weight:178.25
Hs Code.:

Synonyms:2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

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Chemical Property of 2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

Chemical Property:

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Technology Process of 2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

There total 4 articles about 2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1286796-37-9
(2E)-3-mesitylprop-2-en-1-yl 4-nitrobenzoate

: 1286796-46-0
2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

Guidance literature:: With tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl alcohol; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201007307

Reference yield:

: 84001-90-1
(E)-ethyl 3-mesitylacrylate

: 1286796-46-0
2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / toluene / -78 - 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl alcohol / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl alcohol; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/anie.201007307

Reference yield:

: 487-68-3
mesytaldehyde

: 1286796-46-0
2-[(1E)-3-fluoroprop-1-en-1-yl]-1,3,5-trimethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene / 16 h / Reflux; Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / -78 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl alcohol / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; diisobutylaluminium hydride; triethylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl alcohol; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/anie.201007307