2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde

Base Information

Chemical Name:2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde
CAS No.:1245906-83-5
Molecular Formula:C₂₆H₄₈O₅Si₂
Molecular Weight:496.835
Hs Code.:

Synonyms:2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde

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Chemical Property of 2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde

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Technology Process of 2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde

There total 1 articles about 2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1245906-82-4
1-[3,3-bis-(tert-butyl-dimethyl-silanyloxymethyl)-pent-4-enyloxymethyl]-4-methoxy-benzene

: 1245906-83-5
2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde

Guidance literature:: 1-[3,3-bis-(tert-butyl-dimethyl-silanyloxymethyl)-pent-4-enyloxymethyl]-4-methoxy-benzene; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1080/15257770903396725

Reference yield: 86.0%

: 1245906-83-5
2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde

: 75-16-1
methylmagnesium bromide

: 1245906-84-6
3,3-bis-(tert-butyl-dimethyl-silanyloxymethyl)-5-(4-methoxy-benzyloxy)pentan-2-ol

Guidance literature:: 2,2-bis-(tert-butyl-dimethyl-silanyloxymethyl)-4-(4-methoxy-benzyloxy)butyraldehyde; methylmagnesium bromide; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water; at 20 ℃; Saturated solution;
DOI:10.1080/15257770903396725