Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn

Base Information

Chemical Name:Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn
CAS No.:1134204-89-9
Molecular Formula:C₁₄₀H₁₉₉N₂₁O₄₆
Molecular Weight:2912.23
Hs Code.:

Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn

Synonyms:Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn

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Chemical Property of Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn

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Technology Process of Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn

There total 2 articles about Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 953395-50-1
1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-azido-6''-deoxy-kanamycin A

: 1134204-68-4
Fmoc-Trp-Pra-Pra-Trp-NHBn

: 1134204-89-9
Fmoc-Trp(Boc)-β-alanyl-4-[[1,2,3]-triazol-1-yl-[(1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-(4-β-alanyl-4-[1,2,3]-triazol-1-yl-1,3,6',3''-tetra-N-(tert-butoxycarbonyl)-6''-deoxykanamycin)-6'']-Trp(Boc)-NHBn

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃;
DOI:10.1016/j.bmcl.2010.03.116