2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

Base Information

• Chemical Name: 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol
• CAS No.: 104343-31-9
• Molecular Formula: C₄₃H₄₅NO₇
• Molecular Weight: 687.833

Synonyms:2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

Chemical Property of 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

There total 2 articles about 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol (104343-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / tetrahydrofuran / 1 h / Ambient temperature

With potassium carbonate; In tetrahydrofuran;

DOI:10.1021/jo00230a012

Reference yield:

1,2,6-trideoxy-6-<<(phenylmethoxy)carbonyl>amino>-3,4,5,7-tetrakis-O-(phenylmethyl)-D-gluco-hept-1-enitol (104343-30-8) → 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol (104343-31-9)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/jo00230a012

Reference yield: 100.0%

2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol (104343-31-9) → (2R,3R,4S,5S,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-formyl-piperidine-1-carboxylic acid benzyl ester (137326-04-6)

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide;

DOI:10.1016/S0040-4039(00)79409-3

upstream raw materials:

1,2,6-trideoxy-6-<<(phenylmethoxy)carbonyl>amino>-3,4,5,7-tetrakis-O-(phenylmethyl)-D-gluco-hept-1-enitol

benzyl chloroformate

Downstream raw materials:

2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-β-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

(2R,3R,4S,5S,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-formyl-piperidine-1-carboxylic acid benzyl ester

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