2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

Base Information

Chemical Name:2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol
CAS No.:110205-71-5
Molecular Formula:C₃₅H₃₉NO₅
Molecular Weight:553.698
Hs Code.:

Synonyms:2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

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Chemical Property of 2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

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Technology Process of 2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

There total 2 articles about 2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 104343-31-9
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

: 110205-71-5
2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

Guidance literature:: With cyclohexene; palladium on activated charcoal; In methanol;
DOI:10.1016/S0040-4039(00)79409-3

Reference yield:

: 104343-30-8
1,2,6-trideoxy-6-<<(phenylmethoxy)carbonyl>amino>-3,4,5,7-tetrakis-O-(phenylmethyl)-D-gluco-hept-1-enitol

: 110205-71-5
2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

Guidance literature:: Multi-step reaction with 2 steps

2: 83 percent / cyclohexene / 10percent Pd/C / ethanol / 48 h

With cyclohexene; palladium on activated charcoal; In ethanol;
DOI:10.1021/jo00230a012

Reference yield:

: 110205-71-5
2,6-dideoxy-2,6-imino-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

: 137326-16-0
[1S-(1α,2β,3α,4β,9α,9aβ) ]-octahydro-4-(hydroxymethyl)-2H-quinolizine-1,2,3,9-tetrol 9-benzoate

Guidance literature:: Multi-step reaction with 9 steps

1: Et₃N

2: AlH₃ / tetrahydrofuran

3: (COCl)2, DMSO

4: diethyl ether

5: DMAP

6: 1) BH₃*Me₂S 2) H₂O₂

7: cyclohexene / Pd(OH)2 / methanol

8: MsCl, pyridine

9: 85 percent / H₂ / Pd-black / acetic acid

With pyridine; aluminium hydride; dmap; oxalyl dichloride; dimethylsulfide borane complex; hydrogen; dihydrogen peroxide; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; cyclohexene; palladium dihydroxide; palladium; In tetrahydrofuran; methanol; diethyl ether; acetic acid;
DOI:10.1016/S0040-4039(00)79409-3