phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:847237-49-4
Molecular Formula:C₅₃H₄₆O₁₆
Molecular Weight:938.939
Hs Code.:

Synonyms:phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 6 articles about phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 847237-48-3
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-3,4-O-isopropylidene-β-D-galactopyranosyl)-β-D-glucopyranoside

: 847237-49-4
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: In water; acetic acid; at 95 ℃; for 1h;
DOI:10.1016/j.carres.2004.11.017

Reference yield:

: 34361-44-9
phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-2,3,6-tri-O-acetyl-α-D-glucopyranoside

: 847237-49-4
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 9.8 g / NaOMe / methanol / 20 °C

2: 3.0 g / H₂SO₄ / dimethylformamide; acetone / 1 h / Heating

3: 5.86 g / pyridine / 3 h / 20 °C

4: 89 percent / acetic acid; H₂O / 1 h / 95 °C

With sulfuric acid; sodium methylate; In pyridine; methanol; water; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.carres.2004.11.017

Reference yield:

: 3616-19-1,5328-50-7,5346-90-7,6291-42-5,6920-00-9,20764-63-0,20880-60-8,20880-65-3,22352-19-8,23973-20-8,32447-69-1,34213-32-6,52554-32-2,53956-64-2,56907-29-0,56994-12-8,56994-13-9,57128-38-8,67650-36-6,68036-17-9,68036-19-1,78215-50-6,78215-51-7,79549-48-7,80446-82-8,85249-04-3,93221-83-1,93779-27-2,111407-83-1,111407-84-2,111407-85-3,120328-65-6,123809-59-6,132341-46-9,132341-47-0,132341-49-2,145307-94-4
1',2',3',6',2,3,4,6-octa-O-acetyl-β-D-lactose

: 847237-49-4
phenyl 2,3,6-tri-O-benzoyl-4-O-(2,6-di-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / molecular sieves 4 Angstroem; boron trifluoride etherate / CH₂Cl₂

2: 9.8 g / NaOMe / methanol / 20 °C

3: 3.0 g / H₂SO₄ / dimethylformamide; acetone / 1 h / Heating

4: 5.86 g / pyridine / 3 h / 20 °C

5: 89 percent / acetic acid; H₂O / 1 h / 95 °C

With 4 A molecular sieve; sulfuric acid; boron trifluoride diethyl etherate; sodium methylate; In pyridine; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.carres.2004.11.017