3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

Base Information

Chemical Name:3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene
CAS No.:82939-75-1
Molecular Formula:C₁₆H₂₆O₃
Molecular Weight:266.381
Hs Code.:

Synonyms:3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

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Technology Process of 3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

There total 10 articles about 3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 82939-70-6
3-(2-ethylbut-1-en-4-yl)-3-hydroxymethyl-2,4-dimethoxycyclohexa-1,4-diene

: 74-88-4
methyl iodide

: 82939-75-1
3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

Guidance literature:: With sodium hydride; at 50 ℃; for 1.5h;

Reference yield:

: 82939-66-0
methyl 2,6-dimethoxy-2,5-cyclohexadiene-1-carboxylate

: 82939-75-1
3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (i-Pr)2NLi / 1.) THF, hexane, 0 deg C, 5 min, 2.) 0 deg C, 12 h

2: 99.5 percent / LiAlH₄ / diethyl ether / 0.75 h / Ambient temperature

3: 70 percent / NaH / 1.5 h / 50 °C

With lithium aluminium tetrahydride; sodium hydride; lithium diisopropyl amide; In diethyl ether;

Reference yield:

: 82939-71-7
2-Ethyl-4-iodobut-1-ene

: 82939-75-1
3-(2-ethylbut-1-en-4-yl)-2,4-dimethoxy-3-methoxymethylcyclohexa-1,4-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) (i-Pr)2NLi / 1.) THF, hexane, 0 deg C, 5 min, 2.) 0 deg C, 12 h

2: 99.5 percent / LiAlH₄ / diethyl ether / 0.75 h / Ambient temperature

3: 70 percent / NaH / 1.5 h / 50 °C

With lithium aluminium tetrahydride; sodium hydride; lithium diisopropyl amide; In diethyl ether;