1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

Base Information

Chemical Name:1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate
CAS No.:73159-29-2
Molecular Formula:C₃₁H₃₇ClO₁₇
Molecular Weight:717.078
Hs Code.:

Synonyms:1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

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Chemical Property of 1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

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Technology Process of 1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

There total 4 articles about 1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 73159-28-1
3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose 2-chlorosulphate

: 73159-29-2
1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

Guidance literature:: With lithium chloride; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 80 ℃; for 24h;
DOI:10.1016/S0008-6215(00)83670-8

Reference yield:

: 71143-87-8
3,4,6,3',4',6'-hexa-O-acetylsuccrose

: 73159-29-2
1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 38 percent / pyridine; CHCl₃ / 2 h / -50 °C

2: 91 percent / sulphuryl chloride / pyridine; CHCl₃ / 3 h / -70 °C

3: 49 percent / LiCl / hexamethylphosphoric acid triamide / 24 h / 80 °C

With sulfuryl dichloride; lithium chloride; In pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; chloroform;
DOI:10.1016/S0008-6215(00)83670-8

Reference yield:

: 73159-27-0
3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

: 73159-29-2
1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / sulphuryl chloride / pyridine; CHCl₃ / 3 h / -70 °C

2: 49 percent / LiCl / hexamethylphosphoric acid triamide / 24 h / 80 °C

With sulfuryl dichloride; lithium chloride; In pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; chloroform;
DOI:10.1016/S0008-6215(00)83670-8