3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

Base Information

Chemical Name:3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose
CAS No.:73159-27-0
Molecular Formula:C₃₁H₃₈O₁₈
Molecular Weight:698.632
Hs Code.:

Synonyms:3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

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Chemical Property of 3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

Chemical Property:

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Technology Process of 3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

There total 1 articles about 3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 71143-87-8
3,4,6,3',4',6'-hexa-O-acetylsuccrose

: 98-88-4
benzoyl chloride

: 73159-27-0
3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

: 73159-26-9
2,1'-di-O-benzoylsucrose hexa-acetate

Guidance literature:: In pyridine; chloroform; at -50 ℃; for 2h;
DOI:10.1016/S0008-6215(00)83670-8

Reference yield: 91.0%

: 73159-27-0
3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

: 73159-28-1
3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose 2-chlorosulphate

Guidance literature:: With sulfuryl dichloride; In pyridine; chloroform; at -70 ℃; for 3h;
DOI:10.1016/S0008-6215(00)83670-8

Reference yield:

: 73159-27-0
3,4,6,3',4',6'-hexa-O-acetyl-1'-O-benzoylsucrose

: 73159-29-2
1'-O-benzoyl-2-chloro-2-deoxy-manno-sucrose hexa-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / sulphuryl chloride / pyridine; CHCl₃ / 3 h / -70 °C

2: 49 percent / LiCl / hexamethylphosphoric acid triamide / 24 h / 80 °C

With sulfuryl dichloride; lithium chloride; In pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; chloroform;
DOI:10.1016/S0008-6215(00)83670-8